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Phase Engineering, Structural Characterization of 1T-MS2 (M=W/Mo) and Their Energy Applications

Abstract第5-6页
Chapter 1. Introduction and Literature Review第17-52页
    1.1 Background第17-18页
    1.2 The Crystal Structure of (Molybdenum/Tungsten) Disulfide第18-20页
    1.3 Metal Phase (Molybdenum/Tungsten) Disulfide Preparation Methods第20-31页
        1.3.1 High-Pressure Method第20-22页
        1.3.2 Colloidal Synthesis Method第22-23页
        1.3.3 Atomic Plane Gliding Method第23-26页
        1.3.4 Alkali Metal Intercalation Exfoliation Method第26-30页
        1.3.5 Noble Metal Electron Transfer Method第30-31页
    1.4 Metallic Phase (Molybdenum /Tungsten) Disulfide Applications第31-42页
        1.4.1 Supercapacitor Applications第31-35页
        1.4.2 Photocatalytic Hydrogen Production第35-39页
        1.4.3 Electrocatalytic Hydrogen Evolution Reaction第39-42页
    1.5 X-ray Absorption Fine Structure (XAFS) Spectroscopy and Application第42-46页
    1.6 Motiavtion of This Thesis第46-48页
    1.7 References第48-52页
Chapter 2. Metallic 1T-WS_2 Nanoribbons as High Conductive Electrode for Supercapacitor第52-68页
    2.1 Introduction第52-53页
    2.2 Experimental第53-55页
        2.2.1 Hydrothermal Synthesis of Metallic 1T-WS_2 Nanoribbons第53页
        2.2.2 Characterizations第53-54页
        2.2.3 Electrochemical Measurments第54-55页
    2.3 Results and discussion第55-66页
        2.3.1 Morphology第55-57页
        2.3.2 Structural Characterization第57-62页
        2.3.3 Electrochemical Performance第62-66页
    2.4 References第66-68页
Chapter 3. In-situ Integrating Metallic 1T-MoS_2@CdS Heterostructure for Promoted Visible-Light-Driven Photocatalytic Hydrogen Evolution第68-87页
    3.1 Introduction第68-69页
    3.2 Experimental第69-72页
        3.2.1 Synthesis of 1T-MoS_2@CdS Heterostructures第69-70页
        3.2.2 Characterizations第70页
        3.2.3 Photocatalytic Hydrogen Evolution Measurements第70-71页
        3.2.4 Details of the Pump-Probe Experiments第71-72页
    3.3 Results and discussion第72-85页
        3.3.1 Morphology第72-74页
        3.3.2 Structural Characterization第74-78页
        3.3.3 Optical Properties第78-81页
        3.3.4 Photocatalytic Performance第81-85页
    3.4 References第85-87页
Chapter 4. Synthesis of Layered Ni_9S_8/MoS_2 Hetero-catalyst for Enhanced Hydrogen Evolution Reaction第87-99页
    4.1 Introduction第87-89页
    4.2 Experimental第89-90页
        4.2.1 Synthesis of MoS_2 Nanosheets第89页
        4.2.2 Synthesis of the Ni_9S_8/MoS_2 Hybrid第89页
        4.2.3 Photocatalytic Hydrogen Evolution Measurements第89-90页
        4.2.4 Characterizations第90页
    4.3 Results and discussion第90-97页
        4.3.1 Morphology第90-92页
        4.3.2 Structural Characterization第92-94页
        4.3.3 Photocatalytic Performance第94-97页
    4.4 References第97-99页
Chapter 5. Summary and Future Prospects第99-102页
List of Publications第102-104页
Acknowledgement第104-105页

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