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Preparation and Study of Sol-Gel Derived Coatings for Heat Dissipation and Insulation Applications

Abstract第3页
ACKNOWLEDGEMENT第7-9页
ABBREVIATIONS第9-16页
CHAPTER 1:INTRODUCTION第16-40页
    1.1 GENERAL INTRODUCTION第16页
    1.2 THERMAL DISSIPATION COATINGS第16-17页
    1.3 THERMAL INSULATION COATINGS第17-18页
    1.4 THE SOL GEL PROCESS第18-24页
        1.4.1 Introduction第18-20页
        1.4.2 Mechanism of the hydrolysis and condensation reactions of silicon alkoxides第20-22页
        1.4.3 Hydrolysis and condensation of Organosilanes第22-23页
        1.4.4 Hydrolysis and condensation of Titanium compounds第23-24页
        1.4.5 The Datec Sol-gel composite coating第24页
    1.5 SURFACE TREATMENT WITH SILANE COUPLING AGENTS第24-26页
        1.5.1 Functions of coupling agents第25页
        1.5.2 The silane bond to the inorganic substrate第25-26页
        1.5.3 The silane bond to the polymer第26页
    1.6 ORGANIC-INORGANIC HYBRID COATING MATERIALS第26-30页
        1.6.1 Introduction第26-27页
        1.6.2 Types of organic-inorganic hybrids第27-28页
        1.6.3 Epoxy/silica Hybrid coating materials第28-30页
    1.7 THE THEORY OF THERMAL TRANSFER IN COATINGS第30-31页
    1.8 EFFECT OF MICROSTRUCTURE ON THE THERMAL TRANSFER PROPERTIES OF COATINGS第31-33页
    1.9 THERMAL TRANSFER TESTING第33-39页
        1.9.1 Steady state methods of measuring thermal transfer of coatings第33-35页
        1.9.2 Transient Methods第35-39页
    1.10 DESIGN OF EXPERIMENTS第39-40页
CHAPTER 2:HEAT DISSIPATION COATINGS第40-65页
    2.1 INTRODUCTION第40页
    2.2 EXPERIMENTAL DESIGN AND PROCESS第40-47页
        2.2.1 Design of Experiments: The Taguchi approach第40-41页
        2.2.2 Materials第41-42页
        2.2.3 Preparation of sol solutions第42-43页
        2.2.4 Preparation and deposition of coatings第43页
        2.2.5 Characterization and testing第43-47页
    2.3 RESULTS AND DISCUSSION第47-64页
        2.3.1 Taguchi Analysis第47-51页
        2.3.2 Thermal Transfer Properties第51-56页
        2.3.3 Surface morphology第56-59页
        2.3.4 FTIR spectrum第59-61页
        2.3.5 Thermal Analysis (TGA)第61-62页
        2.3.6 Thermal cycling第62-64页
    CONCLUSION第64-65页
CHAPTER 3:HEAT INSULATION COATINGS第65-83页
    3.1 INTRODUCTION第65页
    3.2 EXPERIMENTAL第65-69页
        3.2.1 Materials第65-66页
        3.2.2 Surface modification of hollow glass beads第66-67页
        3.2.3 Preparation of coating solution第67页
        3.2.4 Deposition第67页
        3.2.5 Testing and characterization第67-69页
    3.3 RESULTS AND DISCUSSION第69-81页
        3.3.1 Effect of hollow glass beads content on thermal transfer第69-70页
        3.3.2 Temperature dependence of thermal insulation properties第70-71页
        3.3.3 Effect of coating thickness on thermal transfer properties第71-72页
        3.3.4 Effect of HGM on the mechanical properties第72-74页
        3.3.5 Chemical resistance第74-75页
        3.3.6 FTIR spectroscopy第75-76页
        3.3.7 Surface morphology第76-80页
        3.3.8 Thermogravimetric analysis第80-81页
    3.4 CONCLUSION第81-83页
CHAPTER 4:HEAT TRANSFER MODEL第83-89页
    4.1 INTRODUCTION第83页
    4.2 BOUNDARY AND INITIAL CONDITIONS第83-86页
    4.3 DISCUSSION第86-87页
    4.4 CONCLUSION第87-89页
CHAPTER 5:CONCLUSION AND RECOMMENDATIONS第89-91页
REFERENCES第91-98页
APPENDIX第98-100页
    Ⅰ.List of Academic Publications第98-99页
    Ⅱ.Infrared emissivity Test Reports第99-100页

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