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聚合物前驱体法制备碳化硼粉体的研究

ABSTRACT第8-9页
CHPTER 1 INTRODUCTION第10-35页
    1.1 Introduction to Boron Carbide第10-11页
    1.2 Structure of Boron Carbide第11-13页
    1.3 Application of Boron Carbide第13-15页
    1.4 Synthesis of Boron Carbide第15-32页
        1.4.1 Carbothermic Reduction第16-20页
        1.4.2 Magnesiothermic Reduction第20-21页
        1.4.3 Synthesis from Elements第21-22页
        1.4.4 Chemical Vapor Deposition第22-23页
        1.4.5 Synthesis from Polymeric/ Organic Precursors第23-32页
    1.5 The Proposed Study第32-34页
    1.6 Aim and Objectives of Work第34-35页
CHAPTER 2 SYNTHESIS OF B_4C BY A CONDENSATION REACTION (CR)第35-56页
    2.1 Introduction第35-36页
    2.2 Materials and Equipment第36-37页
    2.3 Synthesis Procedure第37-38页
    2.4 Characterization Techniques第38-39页
        2.4.1 Fourier Transform Infrared Spectroscopy (FTIR)第38-39页
        2.4.2 Thermogravimetric Analysis (TGA)第39页
        2.4.3 X-Ray Diffraction (XRD)第39页
        2.4.4 Scanning Electron Microscope (SEM)第39页
    2.5 Results and Discussions第39-54页
        2.5.1 FTIR Analysis of a PVA, BA, and PVBO第39-41页
        2.5.2 TGA Analysis of a PVA, BA, and PVBO第41-42页
        2.5.3 XRD Analysis of the Synthesized B_4C第42-53页
        2.5.4 SEM Analysis of the Synthesized B_4C第53-54页
    2.6 Conclusion第54-56页
CHAPTER 3 SYNTHESIS OF B_4C BY A SOLID-STATE REACTION (SSR)第56-67页
    3.1 Introduction第56-57页
    3.2 Materials and Equipment第57页
    3.3 Synthesis Procedure第57-58页
    3.4 Characterization Techniques第58-59页
        3.4.1 Fourier Transform Infrared Spectroscopy (FTIR)第58-59页
        3.4.2 X-Ray Diffraction (XRD)第59页
        3.4.3 Scanning Electron Microscope (SEM)第59页
    3.5 Results and Discussions第59-66页
        3.5.1 FTIR Analysis of a PVBO and Preceramic Precursor第59-61页
        3.5.2 XRD Analysis of the Synthesized B_4C第61-64页
        3.5.3 SEM Analysis of the Synthesized B_4C第64-66页
    3.6 Conclusion第66-67页
CHAPTER 4 SYNTHESIS OF B_4C BY A SOLID-STATE REACTION-PYROLYSIS PROCESS (SRPP)第67-79页
    4.1 Introduction第67-68页
    4.2 Materials and Equipment第68页
    4.3 Synthesis Procedure第68-70页
    4.4 Characterization Techniques第70页
        4.4.1 X-Ray Diffraction (XRD)第70页
        4.4.2 Scanning Electron Microscope (SEM)第70页
    4.5 Results and Discussions第70-78页
        4.5.1 XRD Analysis of the Synthesized B_4C第70-76页
        4.5.2 SEM Analysis of the Synthesized B_4C第76-78页
    4.6 Conclusion第78-79页
CHAPTER 5 SYNTHESIS OF B_4C BY A SOLID-STATE POLYMERIZATION (SSR)第79-92页
    5.1 Introduction第79-80页
    5.2 Materials and Equipment第80页
    5.3 Synthesis Procedure第80-81页
    5.4 Characterization Techniques第81-82页
        5.4.1 Fourier Transform Infrared Spectroscopy (FTIR)第81-82页
        5.4.2 X-Ray Diffraction (XRD)第82页
        5.4.3 Scanning Electron Microscope (SEM)第82页
        5.4.4 Particle Size Analysis (PSA)第82页
    5.5 Results and Discussions第82-91页
        5.5.1 FTIR Analysis of a PVBO第82-83页
        5.5.2 XRD Analysis of the Synthesized B_4C第83-87页
        5.5.3 SEM Analysis of the Synthesized B_4C第87-89页
        5.5.4 Particle Size Analysis (PSA) of the Synthesized B_4C第89-91页
    5.6 Conclusion第91-92页
CHAPTER 6 CONCLUSION第92-93页
REFERENCES第93-105页
PUBLICATIONS第105-106页
ACKNOWLEDGEMENT第106页

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