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石墨烯/层状双氢氧化物(LDHs)纳米复合材料及其应用程序作为超级电容器的电极材料

学位论文数据集第4-7页
ABSTRACT第7-8页
摘要第9-16页
CHAPTER 1 GENERAL INTRODUCTION第16-54页
    1.1 THE DEVELOPMENT OF CARBON MATERIALS第16-17页
    1.2 STRUCTURE OF GRAPHENE第17-18页
    1.3 PROPERTIES OF GRAPHENE第18-19页
    1.4 PREPARATION METHOD OF GRAPHENE第19-25页
        1.4.1 Mechanical Stripping Method第19-20页
        1.4.2 Chemical Vapor Deposition Method第20-21页
        1.4.3 Epitaxial Growth Method第21-22页
        1.4.4 Oxidation-Reduction Method第22-24页
        1.4.5 Organic Synthesis第24-25页
        1.4.6 Carbo Nanotube Shear Method第25页
    1.5 APPLICATION OF GRAPHENE第25-29页
        1.5.1 Graphene in the Application of Photovoltaic Devices第26-27页
        1.5.2 Graphene in the Application of Supercapacitor第27-28页
        1.5.3 The Application of Graphene in Fuel Cells第28页
        1.5.4 Graphene in the Application of Photocatalysis第28-29页
    1.6 Layered double Hydroxides第29-31页
    1.7 Structure characteristics of LDH第31-35页
        1.7.1 LDH crystal structure description第31-32页
        1.7.2 The Chemical Composition Of Body Layer Board第32-33页
        1.7.3 Object Interlayer Anionic Species第33-35页
        1.7.4 The Particle Size and Distribution第35页
        1.7.5 Subject Layer Board And Molecular Interactions Between Objects And Layers第35页
    1.8 THREE MAIN PROPERTIES OF LDH第35-36页
        1.8.1 Acid Base Double Function第35页
        1.8.2 Ions Between The Layers Of Exchangeability第35-36页
        1.8.3 Thermal Stability第36页
        1.8.4 Memory Effect第36页
    1.9 SYNTHESIS OF LDH第36-41页
        1.9.1 Coprecipitation Method第36-39页
        1.9.2 ION EXCHANGE METHOD第39页
        1.9.3 Hydrothermal Synthesis Method第39-40页
        1.9.4 Microwave Synthesis第40页
        1.9.5 Roasting Recovery Method第40页
        1.9.6 Back Mixing /Precipitation第40-41页
        1.9.7 The Second Assembly Method第41页
    1.10 Overview of the development of Super capacitor第41-54页
        1.10.1 Supercapacitor Classification第41-42页
        1.10.2 Super capacitor Energy Storage Mechanism第42-45页
        1.10.3 The Characteristics of Supercapacitors第45-46页
        1.10.4. Supercapacitor Assembly and Testing第46-50页
        1.10.5 The Research Progress of Supercapacitor Electrode Materials第50-51页
        1.10.6 The super capacitor Transition metal Compounds第51-54页
CHAPTER 2 MATERIALS CHARACTERIZATION第54-64页
    2.1 MATERIALS AND CHEMICALS第54-56页
    2.2 MATERIALS SYNTHESIS第56-57页
        2.2.1 In-situ Reduction第56页
        2.2.2 Co-precipitation第56页
        2.2.3 Hydrothermal and Solvothermal第56-57页
        2.2.4 Simple Incorporation第57页
    2.3 MATERIALS CHARACTERIZAT:CN第57-64页
        2.3.1 X-ray Diffractometry第57-58页
        2.3.2 Scanning Electron Microscopy and Transmission Electron Microscopy第58-60页
        2.3.3 Raman Spectroscopy第60-61页
        2.3.4 Brunauer-Emmett-Teller Surface Area and Barrett-JoynerHalenda PoreSize and Volume Analysis第61-62页
        2.3.5 Thermogravimetric Analysis第62-64页
CHAPTER 03 ELECTRODE FABRICATION AND CELL ASSEMBLY第64-70页
    3.1 ELECTRODE FABRICATION第64页
    3.2 CELL ASSEMBLY第64-65页
    3.3 ELECTROCHEMICAL TESTING第65-70页
        3.3.1 Cyclic Voltommetry第66-67页
        3.3.2 Galvanostatic Charge/Discharge第67-68页
        3.3.3 Electrochemical Impedance Spectroscopy第68-70页
CHAPTER 4 SYNTHESIS OF GRAPHENE/NI-AL LAYERED DOUBLE HYDROXIDE NANOWIRES AND THEIR APPLICATION AS ELECTRODE MATERIAL FOR SUPERCAPACITORS第70-92页
    4.1 INTRODUCTION第70-72页
    4.2 EXPERIMENTAL AND CHARACTERIZATION第72-74页
        4.2.1 Synthesis第72页
        4.2.2 Preparation of Supercapacitors第72-73页
        4.2.3 Characterization Methods第73-74页
    4.3 RESULTS AND DISCUSSIONS第74-89页
    4.4 CONCLUSION第89-92页
CHAPTER 05第92-94页
    5.1 CONCLUSION第92-94页
References第94-108页
Acknowledgement第108-110页
List of Publication第110-111页
附件第111-112页

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