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A Study on the Morphology of Electrospun Bombyx Mori Fibers and the Secondary Structure of Regenerated Silk Fibroin

ACKNOWLEDGMENT第6-7页
ABSTRACT第7-8页
Contents第9-11页
LIST OF FIGURES第11-12页
LIST OF TABLES第12-13页
LIST OF ABBREIATIONS第13-14页
CHAPTER 1:INTRODUCTION第14-17页
    1.0 INTRODUCTION第14-17页
CHAPTER 2:BACKGROUND AND LITERATURE REVIEW第17-38页
    2.1 Overview of Sericulture第17-18页
    2.2 Properties of Silk第18-21页
        2.2.1 Physical nature of silk第18-20页
        2.2.2 Chemical Behavior of Silk第20-21页
    2.3 Primary Structure of BombyxMori Silk第21-25页
        2.3.1 Sequence in B.Mori Fibroin Structure第24-25页
    2.4 The Secondary Structure of Silk Fibroin第25-30页
        2.4.1 FTIR Conformations in Silk Fibroin第27-30页
            2.4.1.1 FTIR of Regenerated Fibroin第28-30页
        2.4.2 Silk fibroin and X-ray Diffraction第30页
    2.5 Nanofibers第30-31页
    2.6 Electrospun Nanofibers第31-36页
        2.6.1 Electrospinning B.Mori silk第33-35页
        2.6.2 Characterization of Nanofibers第35-36页
    2.7 Problem Statement第36页
    2.8 Research purpose第36-38页
        2.8.1 Objectives第36-38页
CHAPTER 3: MATERIALS AND METHODS第38-42页
    3.1 Materials第38页
    3.2 Silk Dissolution and Preparation SF Films第38-39页
    3.3 Preparation of the Spinning Dope and Electrospinning第39页
    3.4 Structural Characterization of Regenerated Fibroin and Nanofiber Morphology第39-42页
        3.4.1 Scanning Electron Microscopy (SEM)第39-41页
        3.4.2 Fourier Transform Spectroscopy and Wide Angle X-Ray Diffraction第41-42页
CHAPTER 4:RESULTS AND DISCUSSION第42-54页
    4.1 Silk Fiber Dissolution, Dialysis and Electrospinning第42页
    4.2 Nanofiber Morphology by SEM第42-45页
    4.3 FTIR Spectroscopy第45-50页
        4.3.1 Degummed Silk Fibroin (DS)第47-48页
        4.3.2 LiBr Derived Silk Fibroin Film (SFLiBr)第48页
        4.3.3 CaCl_2 Derived Silk Fibroin Film (SFCaCl_2)第48-49页
        4.3.4 SFLiBr Electrospun Silk Fibroin (ESLiBr)第49页
        4.3.5 SFCaCl_2 Electrospun Silk Fibroin (ESCaCl_2)第49-50页
    4.4 Wide angle x-ray diffraction (WAXD) structural analysis第50-54页
CHAPTER 5:CONCLUSIONS AND RECOMMENDATIONS第54-56页
    5.1 Conclusions第54-55页
    5.2 Areas for Further Study第55-56页
REFERENCES第56-64页
APPENDIX第64-69页
PUBLISHED PAPERS DURING POSTGRADUATE YEARS第69-70页
ACKNOWLEDGMENT第70页

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