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Preparation and Characteristic of Self-floating Silica

Abstract第6页
摘要第7-11页
CHAPTER 1: LITERATURE REVIEW第11-33页
    1: Introduction第11-33页
        1.1: Historical circumstantial第11-12页
        1.2: Hydrophobic Silica with Surface Modification第12-13页
        1.3: Objectives of this work第13-14页
        1.4: Background of hydrophobic silica by sol-gel process第14-15页
            1.4.1: Sol-gel process for TEOS第14-15页
        1.5: Structure of silica第15-18页
        1.6: Manufacturing of silica第18-21页
            1.6.1: Laboratory Scale and Others Methodology第19-20页
            1.6.2: Back ground of hydrolysis第20-21页
        1.7: Evaluation of Nano-Silica第21-26页
            1.7.1: The aeration and accumulation portents第24-26页
        1.8: The stuffs of silica nano-particles depend upon size第26-28页
            1.8.1: The Mechanical and Thermal Properties第27页
            1.8.2: The Physic-Chemical Properties第27页
            1.8.3: An Optical Properties第27-28页
        1.9: Photo-polymer with background第28-31页
        1.10: A silica filled nanocomposite polymer第31-33页
CHAPTER 2: EXPERIMENTAL TOOLS, TECHNIQUES AND CHARACTERISTIC第33-55页
    2.1: Chemicals and Pre-cursors第33-35页
    2.2 Experimental instruments and tools第35-36页
    2.3: Characterization methods of sample第36-46页
        2.3.1: Surface morphological (SEM and EDX)第36-37页
        2.3.2: Fourier Transformed Infrared (FT-IR)第37-38页
        2.3.3: Transmission electron microscopy (TEM)第38-40页
        2.3.4: Surface Hardness Tester第40-41页
        2.3.5: Glossy meter第41-43页
        2.3.6: Water Contact Angle第43-44页
        2.3.7: Dynamic mechanical analysis第44-46页
    2.8: How hydrophobic character of a surface alters in response to different stimuli第46-55页
        2.8.1: Wettability第46-48页
        2.8.2: Surface Roughness第48-49页
        2.8.3: By chemical modification第49-50页
        2.8.4: Temperature (℃)第50页
        2.8.5: Solvents第50-51页
        2.8.6: Lights第51-52页
        2.8.7: Electric Field第52页
        2.8.8: pH第52-53页
        2.8.9: Effect of Biological Molecules第53-55页
CHAPTER 3: PREPARATION AND CHARACTERISTIC OF SELF-FLOATING SILICA第55-75页
    3.1: Main theme of Work第55-57页
    3.2: Materials and Experimental第57-61页
        3.2.1: Materials第57页
        3.2.2: Synthesis of Octadecyl 2-((3-(triethoxysilyl) propyl) Amino) Acetate (SP)第57-58页
        3.2.3: Preparation of the silica particles第58-59页
        3.2.4: Photo-polymerization第59-61页
    3.3: Characterizations第61-62页
    3.4: Results and discussions第62-75页
        3.4.1: FT-IR第62-63页
        3.4.2: Particle size measurement by SEM第63-66页
        3.4.3: Dynamic Mechanical Analysis第66-67页
        3.4.4: Surface Morphology第67-69页
        3.4.5: Water Contact Angle (e)第69-70页
        3.4.6: Glossy measurement第70-71页
        3.4.7: Surface hardness第71-75页
CONCULSIONS第75-77页
REFERENCES第77-85页
ACKNOWLEDGEMENTS第85-87页
RESUMES第87-89页
LIST OF PUBLICATIONS第89-90页
附件第90-95页

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