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近红外光谱和HPLC-DAD快速检测野生稻、草药和调味料中的多酚类化合物的研究

ACKNOWLEDGEMENTS第5-6页
摘要第6-8页
ABSTRACT第8-9页
CHAPTER I: REVIEW OF THE LITERATURE第13-35页
    1.1 The main classes of polyphenolic compounds第14-18页
        1.1.1 Phenolic acids第15-16页
        1.1.2 Flavonoids第16-17页
        1.1.3 Tannins第17-18页
        1.1.4 Stilbenes and lignans第18页
    1.2 Antioxidant activity of polypenolic components and human health第18-20页
    1.3 Polyphenolic compounds and food quality第20页
    1.4 Sources of polyphenolic compounds第20-21页
    1.5 Antioxidant properties of wild rice第21-22页
    1.6 Antioxidant properties of different herbs and spices第22-26页
    1.7 Near-infrared (NIR) spectroscopy第26-34页
        1.7.1 Theory and features of NIR spectra第28-31页
        1.7.2 Statistical and multivariate calibration第31-32页
        1.7.3 Instrument and industrial requirements第32页
        1.7.4 System considerations第32-34页
    1.8 AIMS OF THE STUDY第34-35页
CHAPTER II Prediction of total phenolics and flavonoids contents in Chinese wild rice(Zizania latifolia) using NIR spectroscopy第35-51页
    2.1 Introduction第35-36页
    2.2 MATERIAL AND METHODS第36-39页
        2.2.1 Rice samples第36页
        2.2.2 Extraction第36页
        2.2.3 Determination of total phenolics content第36页
        2.2.4 Determination of total flavonoids第36页
        2.2.5 NIR analysis第36-39页
    2.3 RESULTS AND DISCUSSION第39-49页
        2.3.1 Spectra investigation第39-40页
        2.3.2 Quantification of total phenolics content with PLS algorithm第40-45页
        2.3.3 Quantification of flavonoids contents with PLS algorithm第45-49页
    2.4 Summary第49-51页
CHAPTER III Antioxidant activity of polyphenolic compounds in pharmaceutical wild herbsand spices第51-59页
    3.1 Introduction第51页
    3.2 Material and methods第51-53页
        3.2.1 Materials第51-52页
        3.2.2 Extraction第52页
        3.2.3 Determination of total phenolic content第52页
        3.2.4 Determination of total flavonoids第52页
        3.2.5 DPPH radical scavenging assay第52页
        3.2.6 Superoxide scavenging activity第52-53页
        3.2.7 Hydroxyl Radical Scavenging assay第53页
        3.2.8 Statistical analysis第53页
    3.3 Results and discussion第53-58页
        3.3.1 Total phenolic acids and flavonoids contents第53-55页
        3.3.2 Antioxidant activity of wild herbs and spices第55-58页
    3.4 Summary第58-59页
CHAPTER IV Quality assessment of wild herbs and spices using HPLC-DAD chromatographyand principal component analysis第59-67页
    4.1 Introduction第59-60页
    4.2 Material and methods第60-61页
        4.2.1 Samples第60页
        4.2.2 Extraction of polyphenolic compounds from herbs and spices第60页
        4.2.3 Quantification of individual polyphenols by HPLC-DAD第60-61页
        4.2.4 Statistical Analysis第61页
    4.3 Results and discussion第61-66页
        4.3.1 HPLC-DAD analysis of phenolic compounds第61-63页
        4.3.2 Principal component analysis of polyphenolic compounds in wild herbs第63-66页
    4.4 Summary第66-67页
CHAPTER V Quality control and prediction of total phenolics and flavonoids contents in wildherbs and spices using NIR spectroscopy.`第67-86页
    5.1 Introduction第67-68页
    5.2 Material and methods第68-72页
        5.2.1 Wild herbs samples第68页
        5.2.2 Reference analysis第68-69页
        5.2.3 NIR analysis第69-72页
    5.3 RESULTS AND DISCUSSION第72-84页
        5.3.1 Spectra analysis第72-73页
        5.3.2 Quantification of total polyphenolic content in wild herbs with PLS algorithms第73-78页
        5.3.3 Quantification of flavonoids content in wild herbs with PLS algorithms第78-84页
    5.4 Summary第84-86页
CONCLUSIONS AND FUTURE WORK第86-89页
    CONCLUSIONS第86-87页
    FUTURE WORK第87-89页
REFERENCES第89-103页
APPENDIX第103-111页
ABBREVIATIONS第111-112页

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