| Abstract | 第1-8页 |
| 摘要 | 第8-10页 |
| Table of Contents | 第10-14页 |
| List of Schemes | 第14-15页 |
| List of Figures | 第15-18页 |
| List of Tables | 第18-21页 |
| CHAPTER 1-INTRODUCTION | 第21-23页 |
| ·Objectives of the Research Work | 第21页 |
| ·Statement of the Problem | 第21-22页 |
| ·Structure of the Thesis | 第22-23页 |
| CHAPTER 2-LITERATURE REVIEW | 第23-64页 |
| ·Introduction | 第23-25页 |
| ·Polyimide Overview | 第25-33页 |
| ·Development History of Polyimides | 第25-26页 |
| ·Characterisitc Properties and Application of Polyimide(PI)Oligomers | 第26-29页 |
| ·Synthesis of Polyimide Oligomers | 第29-32页 |
| ·Major Factors Influencing the Preparation of PIs | 第32-33页 |
| ·Introduction to Resin Matrices and Polyimides as Adhesives | 第33-46页 |
| ·Characteristics,Advantages and Disadvantages of Resin Matrices | 第33-34页 |
| ·Theories of Adhesion | 第34-37页 |
| ·Some Aspects of Various Adhesion Performance Tests | 第37-45页 |
| ·Factors Affecting Polyimide Adhesive Strength | 第45-46页 |
| ·4,4'-Diamino-4"-Hydroxytriphenylmethane (DAHTM) Monomer | 第46-47页 |
| ·Trimellitic Anhydride (TMA) | 第47-48页 |
| ·Polyimide-Epoxy Resin Matrices | 第48-55页 |
| ·Epoxy Resin | 第48-52页 |
| ·Modification of Epoxy Resins | 第52-55页 |
| ·Glass-Fiber Reinforced Composite of Epoxy Resins | 第55-64页 |
| ·Design Flexibility | 第56-59页 |
| ·Tests Done to Characterize Glass-Fiber Reinforced Composites | 第59-64页 |
| CHAPTER 3-EXPERIMENTAL PROCEDURES AND MATERIALS USED | 第64-82页 |
| ·Introduction | 第64-65页 |
| ·Experimental Raw Materials and Equipment | 第65-67页 |
| ·Experimental Raw Materials | 第65-66页 |
| ·Experimental Apparatus | 第66-67页 |
| ·Monomer Synthesis | 第67-69页 |
| ·Synthesis of Aniline Hydrochloride Sale (AHCS) | 第67-68页 |
| ·Synthesis of 4,4'-diamino-4" -hydroxytriphenylmethane (DAHTM) monomer | 第68-69页 |
| ·Characterization of DAHTM Monomer | 第69页 |
| ·Polyimide Oligomer Synthesis | 第69-71页 |
| ·Synthesis of 4,4'-Diamino-4"-Hydroxytriphenylmethane/Trimellitic Anhydrie (CIDAHTM)-Imide Oligomer | 第69-70页 |
| ·Synthesis of 2,2-Bis[4-(4-Aminophenoxy)Phenyl]Propane/Trimellitic Anhydride (CIBAPP)-Imide Oligomer | 第70-71页 |
| ·FT-IR Characterization of Imide Oligomers | 第71页 |
| ·Preparation of the Modified Resin Matrices | 第71-78页 |
| ·Solid CIDAHTM Oligomer and DER 331 E51 Epoxy Resin (P-EP 1 and 2) | 第71-73页 |
| ·Solid CIDAHTM Oligomer and TGDDMEpoxy Resin (P-EP 3) | 第73页 |
| ·CIDAHTM Oligomer Solution and E51 Epoxy Resin (P-EP 4) | 第73-74页 |
| ·CIBAPP Oligomer Solution and Different Ratios of E51 + TGDDM Epoxy Resins (P-EP5, P-EP 6, P-EP 7, P-EP 8 and P-EP 9) | 第74-75页 |
| ·Tests done to characterize Resin Matrices | 第75-78页 |
| ·Preparation of the Glass-Reinforced Composite of Modified Epoxy Resin | 第78-82页 |
| ·Preparation of the Modified Epoxy Resin | 第78页 |
| ·Preparation of the Glass-Fabric | 第78-79页 |
| ·Composite Fabrication | 第79页 |
| ·Tests done to characterize the Composite | 第79-82页 |
| CHAPTER 4-RESULTS AND DISCUSSIONS | 第82-129页 |
| ·DAHTM Monomer Synthesis | 第82-83页 |
| ·Synthesis of Carboxylic Imide Oligomers | 第83-84页 |
| ·CIDAHTM Imide Oligomer | 第83-84页 |
| ·CIBAPP Imide Oligomer | 第84页 |
| ·Preparation of the Modified Resin Matrices | 第84-123页 |
| ·Solid CIDAHTM Imide Oligomer and DER 331 E51 Epoxy Resin | 第85-90页 |
| ·Solid CIDAHTMImide Oligomer and TGDDMEpoxy Resin | 第90-94页 |
| ·CIDAHTM Imide Oligomer Solution and DER 331 E51 Epoxy Resin | 第94-100页 |
| ·CIBAPP Oligomer Solution and Different Ratios of E51 + TGDDM Epoxy Resin | 第100-123页 |
| ·Preparation of Glass-Fiber Reinforced Composite of Modified Epoxy Resin | 第123-129页 |
| ·Dielectric Strength | 第123-124页 |
| ·Volume Resistance | 第124页 |
| ·Longitudinal (0°) and Transverse (90°) Three-Point Bending test | 第124-125页 |
| ·Water Absorption | 第125-126页 |
| ·Contact Angle θ and Surface Energy γ | 第126页 |
| ·Dielectric constant and dielectric loss | 第126-129页 |
| CHAPTER 5-CONCLUSIONS AND RECOMMENDATIONS | 第129-132页 |
| ·Conclusions | 第129-131页 |
| ·Recommendations and Suggested Areas for Further Research | 第131-132页 |
| References | 第132-144页 |
| Published Papers | 第144-145页 |
| Acknowledgements | 第145页 |
