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氧气燃料油的催化氧化脱硫

ABSTRACT第4页
摘要第6-13页
Chapter-1 Introduction and literature第13-33页
    1.1 Environmental background第13页
    1.2 The overview of fuel第13-16页
        1.2.1 General overview第13页
        1.2.2 Diesel fuel第13-16页
        1.2.3 Sulfur regulations第16页
    1.3 Classification of desulfurization technologies第16-31页
        1.3.1 Hydro-desulfurization第18-21页
        1.3.2 Adsorption desulfurization第21-24页
        1.3.3 Oxidative desulfurization第24-31页
    1.4 The objective of this research第31-33页
Chapter-2 Experimental materials, analysis methods and preparation of model oils第33-43页
    2.1 Chemicals and raw materials第34页
    2.2 Preparation of different Model oils第34-35页
        2.2.1 Preparation of n-octane DBT第35页
        2.2.2 Preparation of CH3CN DBT第35页
    2.3 General description of desulfurization process第35-37页
        2.3.1 Oxidative desulfurization of DBT oil第35-36页
        2.3.2 Adsorptive desulfurization of DBT oil第36-37页
    2.4 Experiments design, setup and process descriptions第37-39页
        2.4.1 Catalyst loaded with activated carbon第37页
        2.4.2 Catalyst with acetic acid and HBr第37-38页
        2.4.3 MOFs as a catalyst第38页
        2.4.4 Oxidative desulfurization of DBT oil (CH3CN)第38页
        2.4.5 Oxidative desulfurization of DBT oil(n-octane)第38-39页
        2.4.6 Oxidation with pure n-octane第39页
    2.5 Analytical methods第39-43页
        2.5.1 Analytical instruments第39-43页
Chapter-3 Catalyst preparation and characterization第43-53页
    3.1 Catalyst loading with activated carbon第43-44页
        3.1.1 Cobalt acetate第43页
        3.1.2 Manganese acetate第43页
        3.1.3 Ferric chloride and Vanadium pentoxide第43-44页
    3.2 Preparation of MOFs第44-46页
        3.2.1 Cobalt MOF第44-45页
        3.2.2 Manganese MOF第45页
        3.2.3 Cobalt&Manganese MOF第45-46页
        3.2.4 Copper MOF第46页
    3.3 Characterization第46-53页
        3.3.1 Scanning Electron Microscopy SEM第46-50页
        3.3.2 X-ray Diffraction (XRD)第50-53页
Chapter-4 Adsorptive and oxidative behavior of catalysts and other compounds第53-69页
    4.1 Adsorptive behavior of MOFs第53-54页
    4.2 Oxidative behavior of catalysts第54-56页
        4.2.1 ODS with catalyst loaded on activated carbon第54-55页
        4.2.2 ODS with catalyst of acetic acid and HBr第55-56页
    4.3 Oxidative desulfurization using MOFs as catalyst第56-58页
        4.3.1 MOFs with Ionic liquid第56-57页
        4.3.2 MOFs without ionic liquid第57-58页
    4.4 Oxidative desufurization of DBT in CH3CN第58-59页
    4.5 Soluble compounds第59-61页
    4.6 Oxidation of pure n-octane第61-66页
    4.7 Summary第66-69页
Chapter-5 Results and discussion第69-75页
    5.1 Study of MOFs第69-70页
        5.1.1 Activation of MOFs第69页
        5.1.2 Regeneration of MOFs第69页
        5.1.3 Reusability of MOFs第69-70页
    5.2 Effect of process parameter on Co-MOF desulfurization efficiency第70-75页
        5.2.1 Effect of temperature on oxidative desulfurization with Co-MOF catalyst第71页
        5.2.2 Effect of pressure on oxidative desulfurization with Co-MOF catalyst第71-75页
Conclusion第75-77页
References第77-87页
Acknowledgements and dedication第87-89页
Introduction to author and supervisor第89-90页
附件第90-91页

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