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Systematic Studies of Enhanced Physical Properties of Ceramics Graphene Nanostructures Assembly Prepared by Solvothermal/Hydrothermal and Hot-Pressing Process

ABSTRACT第4-6页
List of Abbreviations第17-18页
Chapter 1. Introduction第18-33页
    1.1. Introduction第18-25页
        1.1.1. Background and Motivation第18-25页
    1.2. Objectives第25-26页
    1.3. Thesis Organization第26-29页
    1.4. Reference第29-33页
Chapter 2. Experimental Setup and Characterization Tools第33-38页
    2.1. Experimental Setup/Fabrication Route for this ResearchWork第33-35页
    2.2. Characterization Tools for this Research Work第35-38页
        2.2.1. For Morphological Study of γ-Al_2O_3-rGO and SiO_2-rGO第35页
        2.2.2. For Structural and Elemental Study of γ-Al_2O_3-rGO and SiO_2-rGO第35-36页
        2.2.3. For Physical Properties Study of γ-Al_2O_3-rGO and SiO_2-rGO第36页
        2.2.4. For Statistical Analysis of Nano Structures第36-38页
Chapter 3. Synthesis,Characterization and Physical Propertiesof γ-Al_2O_3 Nanorods and rGO Platelets Hybrids第38-76页
    3.1. Introduction第38-40页
    3.2. Experimental Setup第40-43页
        3.2.1. Preparation of γ-Al_2O_3-rGO Hybrid Powder第40-42页
        3.2.2. Hot press processing of γ-Al_2O_3-rGO hybrids第42页
        3.2.3. Characterization Tools第42-43页
    3.3. Results and Discussions第43-71页
        3.3.1. Thermogravimetric analysis (TGA) of γ-Al_2O_3-rGO第43-44页
        3.3.2. Morphological Analysis of γ-Al_2O_3-rGO第44-45页
        3.3.3. Calcination Effect in Physical Color Change of γ-Al_2O_3-rGO第45-46页
        3.3.4. Structural Study of γ-Al_2O_3-rGO Using X-ray diffraction (XRD)第46-48页
        3.3.5. Structural Analysis of γ-Al_2O_3-rGO by Raman Spectroscopy第48-49页
        3.3.6. Structural study of γ-Al_2O_3-rGO by Brunauer-Emmett-Teller(BET) Curves第49-53页
        3.3.7. Effect of Calcination Conditions on Crystallinity ofγ-Al_2O_3-rGOHybrids第53-54页
        3.3.8. Calcination Temperature Effect on Average Diameter ofAlumina Nano rods第54-55页
        3.3.9. Calcination Temperature Effect on Average Length of AluminaNano Rods第55-57页
        3.3.10. Study of Hot Pressing Experimental Conditions BetweenAlumina and Reduced Graphene Oxide第57-58页
        3.3.11. Study of Hot Pressing Effect on γ-Al_2O_3-rGO Hybrid usingSEM,Raman,and XRD第58-61页
        3.3.12. Electrical Conductivity Measurements of γ-Al_2O_3-rGO and γ-Al_2O_3-rGO Hybrids第61-62页
        3.3.13. Thermal Conductivity Measurements of γ-Al_2O_3 and γ-Al_2O_3 -rGO Hybrids and Effect of Temperature on Thermal Conductivity 613.3.14. Dielectric Properties Measurements of γ-Al_2O_3 and γ-Al_2O_3 -rGO Hybrids and Effect of rGO Content on Dielec第62-63页
        3.3.14. Dielectric Properties Measurements of y-Al_2〇_3and Y-AI_2O_3-rGO Hybrids and Effect of rGO Content on Dielectric Properties第63-65页
        3.3.15. Compressive/Tensile Stress Strain Curves,Young'sModulus Study of γ-Al_2O_3 and γ-Al_2O_3 -rGO Hybrids and Effect ofrGO Content on Mechanical Properties第65-69页
        3.3.16. Comparison of Physical Properties of Hot-Press ProcessedAlumina-rGO Hybrids with Previous Reports第69-71页
    3.4. Summary第71-73页
    3.5. References第73-76页
Chapter 4. Synthesis,Characterization and Physical Propertiesof Solvothermal-Hot Press Processed SiO_2 Nano Spheres-rGOplatelets hybrids第76-115页
    4.1. Introduction第76-80页
    4.2. Experimental Setup第80-82页
        4.2.1. Preparation of SiO_2-rGO hybrid powder第80-81页
        4.2.2. Hotpress processing of SiO_2-rGO hybrid powder第81页
        4.2.3. Characterizations Tools第81-82页
    4.3. Results and Discussion第82-106页
        4.3.1. Physical Color Change of SiO_2-rGO Powde第82-83页
        4.3.2. Thermogravimetric Analysis (TGA) of SiO_2-rGO Powder第83-84页
        4.3.3. Morphological Study of SiO_2-rGO Hybrids using SEM,TEMand SAED第84-87页
        4.3.4. Structural Characterization of SiO_2-rGO Hybrids by X-rayDiffraction第87-88页
        4.3.5. Structural Analysis of SiO_2-rGO using Raman Spectroscopy第88-89页
        4.3.6. Structural Analysis of SiO_2-rGO hybrids using FTIRSpectroscopy第89-91页
        4.3.7. Chemical Composition and Elemental State Study of SiO_2-rGO hybrids using XPS Curves第91-92页
        4.3.8. BET surface area,Mesoporous volume % Study of SiO_2-rGOhybrids第92-94页
        4.3.9. Effect of Calcination Temperature on Crystallinity of SiO_2-rGOhybrid第94-97页
        4.3.10. Effect of Hot Pressing on quality of graphene in SiO_2-rGOhybrids第97-98页
        4.3.11. Study of Limited Chemical Reaction between SiO_2 and rGOin Hot-Press Processing第98-99页
        4.3.12. Electrical Conductivity Measurements of SiO_2-rGO hybridand Effect of rGO Content on SiO_2-rGO hybrids第99-100页
        4.3.13. Thermal Conductivity Measurement of SiO_2-rGO Hybridsand Effect of rGO%第100-102页
        4.3.14. Dielectric Measurements and Effect of % rGO Content inSiO_2-rGO hybrids第102-103页
        4.3.15. Tensile Strength and Young's Modulus of SiO_2-rGO Hybridsand Effect of % rGO Content第103-106页
        4.3.16. Comparison of Hot-Press Processed SiO_2-rGO hybrids withPreviously Published Work第106页
    4.4. Summary第106-110页
    4.5. References第110-115页
Chapter 5. Conclusions第115-118页
Acknowledgement第118-119页
List of Publications第119-122页

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