ABSTRACT | 第4-6页 |
List of Abbreviations | 第17-18页 |
Chapter 1. Introduction | 第18-33页 |
1.1. Introduction | 第18-25页 |
1.1.1. Background and Motivation | 第18-25页 |
1.2. Objectives | 第25-26页 |
1.3. Thesis Organization | 第26-29页 |
1.4. Reference | 第29-33页 |
Chapter 2. Experimental Setup and Characterization Tools | 第33-38页 |
2.1. Experimental Setup/Fabrication Route for this ResearchWork | 第33-35页 |
2.2. Characterization Tools for this Research Work | 第35-38页 |
2.2.1. For Morphological Study of γ-Al_2O_3-rGO and SiO_2-rGO | 第35页 |
2.2.2. For Structural and Elemental Study of γ-Al_2O_3-rGO and SiO_2-rGO | 第35-36页 |
2.2.3. For Physical Properties Study of γ-Al_2O_3-rGO and SiO_2-rGO | 第36页 |
2.2.4. For Statistical Analysis of Nano Structures | 第36-38页 |
Chapter 3. Synthesis,Characterization and Physical Propertiesof γ-Al_2O_3 Nanorods and rGO Platelets Hybrids | 第38-76页 |
3.1. Introduction | 第38-40页 |
3.2. Experimental Setup | 第40-43页 |
3.2.1. Preparation of γ-Al_2O_3-rGO Hybrid Powder | 第40-42页 |
3.2.2. Hot press processing of γ-Al_2O_3-rGO hybrids | 第42页 |
3.2.3. Characterization Tools | 第42-43页 |
3.3. Results and Discussions | 第43-71页 |
3.3.1. Thermogravimetric analysis (TGA) of γ-Al_2O_3-rGO | 第43-44页 |
3.3.2. Morphological Analysis of γ-Al_2O_3-rGO | 第44-45页 |
3.3.3. Calcination Effect in Physical Color Change of γ-Al_2O_3-rGO | 第45-46页 |
3.3.4. Structural Study of γ-Al_2O_3-rGO Using X-ray diffraction (XRD) | 第46-48页 |
3.3.5. Structural Analysis of γ-Al_2O_3-rGO by Raman Spectroscopy | 第48-49页 |
3.3.6. Structural study of γ-Al_2O_3-rGO by Brunauer-Emmett-Teller(BET) Curves | 第49-53页 |
3.3.7. Effect of Calcination Conditions on Crystallinity ofγ-Al_2O_3-rGOHybrids | 第53-54页 |
3.3.8. Calcination Temperature Effect on Average Diameter ofAlumina Nano rods | 第54-55页 |
3.3.9. Calcination Temperature Effect on Average Length of AluminaNano Rods | 第55-57页 |
3.3.10. Study of Hot Pressing Experimental Conditions BetweenAlumina and Reduced Graphene Oxide | 第57-58页 |
3.3.11. Study of Hot Pressing Effect on γ-Al_2O_3-rGO Hybrid usingSEM,Raman,and XRD | 第58-61页 |
3.3.12. Electrical Conductivity Measurements of γ-Al_2O_3-rGO and γ-Al_2O_3-rGO Hybrids | 第61-62页 |
3.3.13. Thermal Conductivity Measurements of γ-Al_2O_3 and γ-Al_2O_3 -rGO Hybrids and Effect of Temperature on Thermal Conductivity 613.3.14. Dielectric Properties Measurements of γ-Al_2O_3 and γ-Al_2O_3 -rGO Hybrids and Effect of rGO Content on Dielec | 第62-63页 |
3.3.14. Dielectric Properties Measurements of y-Al_2〇_3and Y-AI_2O_3-rGO Hybrids and Effect of rGO Content on Dielectric Properties | 第63-65页 |
3.3.15. Compressive/Tensile Stress Strain Curves,Young'sModulus Study of γ-Al_2O_3 and γ-Al_2O_3 -rGO Hybrids and Effect ofrGO Content on Mechanical Properties | 第65-69页 |
3.3.16. Comparison of Physical Properties of Hot-Press ProcessedAlumina-rGO Hybrids with Previous Reports | 第69-71页 |
3.4. Summary | 第71-73页 |
3.5. References | 第73-76页 |
Chapter 4. Synthesis,Characterization and Physical Propertiesof Solvothermal-Hot Press Processed SiO_2 Nano Spheres-rGOplatelets hybrids | 第76-115页 |
4.1. Introduction | 第76-80页 |
4.2. Experimental Setup | 第80-82页 |
4.2.1. Preparation of SiO_2-rGO hybrid powder | 第80-81页 |
4.2.2. Hotpress processing of SiO_2-rGO hybrid powder | 第81页 |
4.2.3. Characterizations Tools | 第81-82页 |
4.3. Results and Discussion | 第82-106页 |
4.3.1. Physical Color Change of SiO_2-rGO Powde | 第82-83页 |
4.3.2. Thermogravimetric Analysis (TGA) of SiO_2-rGO Powder | 第83-84页 |
4.3.3. Morphological Study of SiO_2-rGO Hybrids using SEM,TEMand SAED | 第84-87页 |
4.3.4. Structural Characterization of SiO_2-rGO Hybrids by X-rayDiffraction | 第87-88页 |
4.3.5. Structural Analysis of SiO_2-rGO using Raman Spectroscopy | 第88-89页 |
4.3.6. Structural Analysis of SiO_2-rGO hybrids using FTIRSpectroscopy | 第89-91页 |
4.3.7. Chemical Composition and Elemental State Study of SiO_2-rGO hybrids using XPS Curves | 第91-92页 |
4.3.8. BET surface area,Mesoporous volume % Study of SiO_2-rGOhybrids | 第92-94页 |
4.3.9. Effect of Calcination Temperature on Crystallinity of SiO_2-rGOhybrid | 第94-97页 |
4.3.10. Effect of Hot Pressing on quality of graphene in SiO_2-rGOhybrids | 第97-98页 |
4.3.11. Study of Limited Chemical Reaction between SiO_2 and rGOin Hot-Press Processing | 第98-99页 |
4.3.12. Electrical Conductivity Measurements of SiO_2-rGO hybridand Effect of rGO Content on SiO_2-rGO hybrids | 第99-100页 |
4.3.13. Thermal Conductivity Measurement of SiO_2-rGO Hybridsand Effect of rGO% | 第100-102页 |
4.3.14. Dielectric Measurements and Effect of % rGO Content inSiO_2-rGO hybrids | 第102-103页 |
4.3.15. Tensile Strength and Young's Modulus of SiO_2-rGO Hybridsand Effect of % rGO Content | 第103-106页 |
4.3.16. Comparison of Hot-Press Processed SiO_2-rGO hybrids withPreviously Published Work | 第106页 |
4.4. Summary | 第106-110页 |
4.5. References | 第110-115页 |
Chapter 5. Conclusions | 第115-118页 |
Acknowledgement | 第118-119页 |
List of Publications | 第119-122页 |