| 摘要 | 第1-5页 |
| ABSTRACT | 第5-7页 |
| ACKNOWLEDGEMENTS | 第7-8页 |
| CONTENTS | 第8-10页 |
| LIST OF FIGURE | 第10-12页 |
| LIST OF TABLES | 第12-13页 |
| CHAPTER 1 INTRODUCTION | 第13-35页 |
| ·Research background of this subject | 第13-14页 |
| ·Nanotechnology and hydrogen economy | 第14-18页 |
| ·Producing Hydrogen with Sunlight | 第16-18页 |
| ·Synthesis of nanocrystalline powders | 第18-29页 |
| ·Gas phase synthesis | 第18-20页 |
| ·Plasma chemical technique | 第20-21页 |
| ·Precipitation from colloid solutions | 第21-23页 |
| ·Thermal decomposition and reduction | 第23-24页 |
| ·Milling and mechanical alloying | 第24-25页 |
| ·Synthesis by denotation and electric explosion | 第25-27页 |
| ·Ordering in non-stoichiometer compounds | 第27-28页 |
| ·Synthesis of high-dispersed oxides in liquid metals | 第28-29页 |
| ·Self-propagating high-temperature synthesis | 第29页 |
| ·Sol-GelProcess Steps and Combustion Technique | 第29-35页 |
| CHAPTER 2 EXPERIMENTAL METHOD | 第35-40页 |
| ·Raw materials | 第35页 |
| ·Material synthesis | 第35-36页 |
| ·Materials Characterization | 第36-40页 |
| ·Scanning Electron Microscope (SEM) and Energy Dispersive X-ray spectroscopy (EDX) | 第37-38页 |
| ·X-ray diffraction (XRD) analysis | 第38-39页 |
| ·Thermal analysis | 第39-40页 |
| CHAPTER 3 RESULTS AND DISCUSSION | 第40-71页 |
| ·Introduction | 第40页 |
| ·Preparation of Samples with NiCl_2 and EDTA | 第40-46页 |
| ·Preparation of Samples with Ni(NO_3)_2 and EDTA | 第46-54页 |
| ·Preparation of Samples with Ni(NO_3)_2、NiCl_2 and EDTA | 第54-58页 |
| ·Preparation of Samples with Ni(NO_3)_2、Ni(OAc)_2 and TEA | 第58-63页 |
| ·Preparation of Samples with Ni(NO_3)_2、CA、EG and TEA | 第63-71页 |
| CHAPTER 4 CONCLUSION | 第71-73页 |
| ·Conclusion | 第71-72页 |
| ·Future work | 第72-73页 |
| REFERENCES | 第73-76页 |
