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乙基香兰素结晶过程设计

摘要第3-4页
abstract第4页
Chapter 1 Introduction第8-16页
    1.1 Background第8-12页
    1.2 Ethyl Vanillin(EVA)第12-15页
        1.2.1 Methods of Manufacturing第12-13页
        1.2.2 Use and Applications第13页
        1.2.3 Molecular Structure Determination第13-14页
        1.2.4 Structure-Mechanical Property Relationship第14页
        1.2.5 Crystal Structure第14-15页
    1.3 Aims and Scope第15-16页
Chapter 2 Theoretical Fundamentals第16-42页
    2.1 Solubility of Organic Compounds第16-18页
        2.1.1 Solubility Prediction第16-17页
        2.1.2 Solubility Measurement Methods第17-18页
    2.2 Crystallization Kinetics第18-28页
        2.2.1 Supersaturation第19页
        2.2.2 Nucleation and Crystal Growth第19-21页
        2.2.3 Metastability and Metastable Zone Width(MSZW)第21页
        2.2.4 MSZW Measurements第21-26页
        2.2.5 Crystal Growth Mechanisms第26-28页
    2.3 Turbidity第28页
    2.4 Solubility Curves and Metastable Zones第28-30页
    2.5 Automated Simultaneous Determination of MSZW第30-34页
        2.5.1 Turbidimetry and Nephelometry第30页
        2.5.2 The Temperature Variation(TV)method第30-31页
        2.5.3 Equilibrium Concentration versus Dynamic Methods第31-32页
        2.5.4 CrystalLEYES- A Basic Tool第32-34页
    2.6 Crystalline Form第34-36页
        2.6.1 Particle Size第35-36页
    2.7 Characterization of Crystal Size Distribution第36-37页
        2.7.1 Particle Size Distribution第36-37页
    2.8 Crystal Morphology第37-40页
        2.8.1 Effect of Solvent on Crystal Morphology第37-38页
        2.8.2 Morphology Prediction of Crystals第38-39页
        2.8.3 Computer Prediction of Crystal Morphology第39-40页
    2.9 Some Critical Issues in Crystallization Practice第40-42页
Chapter 3 Experiments第42-52页
    3.1 Background第42页
    3.2 Scope of Experimental Work第42页
    3.3 Problem Description第42-43页
    3.4 Chemical Raw Materials第43-44页
    3.5 Experimental Work Procedures第44-52页
        3.5.1 Detection and Characterization of Crystalline Form第44页
        3.5.3 Determination of Solubility Data第44页
        3.5.4 Solubility and MSZW Measurements第44-48页
        3.5.5 Optimization Experiments第48-52页
Chapter 4 Results and Discussion第52-78页
    4.1 Crystalline Form Results第52-53页
        4.1.1 X-Ray Powder Diffraction第52页
        4.1.2 Differential Scanning Calorimetry第52-53页
    4.2 The Solubility of EVA in Binary Solvent第53-55页
    4.3 Dissolution and Nucleation Temperatures第55-56页
    4.4 Metastable Zone Width of EVA in Binary Solvent第56-59页
        4.4.1 The Dependence ofΔTmax/T0 on the Cooling Rate b第56-58页
        4.4.2 The Effect of Agitation Rate第58-59页
    4.5 Optimization Results and Discussion第59-78页
        4.5.1 Literature Back-up and Strategic Modeling第59-60页
        4.5.2 Results for Raw(Unprocessed)EVA第60-62页
        4.5.3 The Effects of Solvent and Sonication第62-72页
        4.5.4 PVM Morphological Results第72-76页
        4.5.5 Discussion第76-78页
Chapter 5 Conclusions and Suggestions第78-80页
    5.1 Conclusions第78-79页
    5.2 Suggestions第79-80页
References第80-86页
Appendix第86-89页
    Appendix A Analysis of the Experimental MSZW第86-89页
Published Papers and Participated Scientific Research第89-90页
    List of Publications第89页
    Role and Contributions第89-90页
Acknowledgements第90页

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